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In Situ Characterization Of Heterogeneous Catalysts

Author: José A. Rodriguez
Publisher: John Wiley & Sons
ISBN: 1118355911
Size: 73.17 MB
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Helps researchers develop new catalysts for sustainable fuel and chemical production Reviewing the latest developments in the field, this book explores the in-situ characterization of heterogeneous catalysts, enabling readers to take full advantage of the sophisticated techniques used to study heterogeneous catalysts and reaction mechanisms. In using these techniques, readers can learn to improve the selectivity and the performance of catalysts and how to prepare catalysts as efficiently as possible, with minimum waste. In-situ Characterization of Heterogeneous Catalysts features contributions from leading experts in the field of catalysis. It begins with an introduction to the fundamentals and then covers: Characterization of electronic and structural properties of catalysts using X-ray absorption fine structure spectroscopy Techniques for structural characterization based on X-ray diffraction, neutron scattering, and pair distribution function analysis Microscopy and morphological studies Techniques for studying the interaction of adsorbates with catalyst surfaces, including infrared spectroscopy, Raman spectroscopy, EPR, and moderate pressure XPS Integration of techniques that provide information on the structural properties of catalysts with techniques that facilitate the study of surface reactions Throughout the book, detailed examples illustrate how techniques for studying catalysts and reaction mechanisms can be applied to solve a broad range of problems in heterogeneous catalysis. Detailed figures help readers better understand how and why the techniques discussed in the book work. At the end of each chapter, an extensive set of references leads to the primary literature in the field. By explaining step by step modern techniques for the in-situ characterization of heterogeneous catalysts, this book enables chemical scientists and engineers to better understand catalyst behavior and design new catalysts for green, sustainable fuel and chemical production.

Heterogeneous Catalysis At Nanoscale For Energy Applications

Author: Franklin (Feng) Tao
Publisher: John Wiley & Sons
ISBN: 1118843525
Size: 44.33 MB
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This book presents both the fundamentals concepts and latest achievements of a field that is growing in importance since it represents a possible solution for global energy problems. It focuses on an atomic-level understanding of heterogeneous catalysis involved in important energy conversion processes. It presents a concise picture for the entire area of heterogeneous catalysis with vision at the atomic- and nano- scales, from synthesis, ex-situ and in-situ characterization, catalytic activity and selectivity, to mechanistic understanding based on experimental exploration and theoretical simulation. The book: Addresses heterogeneous catalysis, one of the crucial technologies employed within the chemical and energy industries Presents the recent advances in the synthesis and characterization of nanocatalysts as well as a mechanistic understanding of catalysis at atomic level for important processes of energy conversion Provides a foundation for the potential design of revolutionarily new technical catalysts and thus the further development of efficient technologies for the global energy economy Includes both theoretical studies and experimental exploration Is useful as both a textbook for graduate and undergraduate students and a reference book for scientists and engineers in chemistry, materials science, and chemical engineering

Design Of Heterogeneous Catalysts

Author: Umit S. Ozkan
Publisher: John Wiley & Sons
ISBN: 352762533X
Size: 42.28 MB
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This long-awaited reference source is the first book to focus on this important and hot topic. As such, it provides examples from a wide array of fields where catalyst design has been based on new insights and understanding, presenting such modern and important topics as self-assembly, nature-inspired catalysis, nano-scale architecture of surfaces and theoretical methods. With its inclusion of all the useful and powerful tools for the rational design of catalysts, this is a true "must have" book for every researcher in the field.

Heterogeneous Catalysts For Clean Technology

Author: Karen Wilson
Publisher: John Wiley & Sons
ISBN: 3527659005
Size: 75.43 MB
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Reactive, but not a reactant. Heterogeneous catalysts play an unseen role in many of today's processes and products. With the increasing emphasis on sustainability in both products and processes, this handbook is the first to combine the hot topics of heterogeneous catalysis and clean technology. It focuses on the development of heterogeneous catalysts for use in clean chemical synthesis, dealing with how modern spectroscopic techniques can aid the design of catalysts for use in liquid phase reactions, their application in industrially important chemistries - including selective oxidation, hydrogenation, solid acid- and base-catalyzed processes - as well as the role of process intensification and use of renewable resources in improving the sustainability of chemical processes. With its emphasis on applications, this book is of high interest to those working in the industry.

Catalysis By Materials With Well Defined Structures

Author: Zili Wu
Publisher: Academic Press
ISBN: 0128013400
Size: 67.40 MB
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Catalysis by Materials with Well-Defined Structures examines the latest developments in the use of model systems in fundamental catalytic science. A team of prominent experts provides authoritative, first-hand information, helping readers better understand heterogeneous catalysis by utilizing model catalysts based on uniformly nanostructured materials. The text addresses topics and issues related to material synthesis, characterization, catalytic reactions, surface chemistry, mechanism, and theoretical modeling, and features a comprehensive review of recent advances in catalytic studies on nanomaterials with well-defined structures, including nanoshaped metals and metal oxides, nanoclusters, and single sites in the areas of heterogeneous thermal catalysis, photocatalysis, and electrocatalysis. Users will find this book to be an invaluable, authoritative source of information for both the surface scientist and the catalysis practitioner Outlines the importance of nanomaterials and their potential as catalysts Provides detailed information on synthesis and characterization of nanomaterials with well-defined structures, relating surface activity to catalytic activity Details how to establish the structure-catalysis relationship and how to reveal the surface chemistry and surface structure of catalysts Offers examples on various in situ characterization instrumental techniques Includes in-depth theoretical modeling utilizing advanced Density Functional Theory (DFT) methods

Basic Principles In Applied Catalysis

Author: Manfred Baerns
Publisher: Springer Science & Business Media
ISBN: 3662059819
Size: 73.12 MB
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Written by a team of internationally recognized experts, this book addresses the most important types of catalytic reactions and catalysts as used in industrial practice. Both applied aspects and the essential scientific principles are described. The main topics can be summarized as follows: heterogeneous, homogeneous and biocatalysis, catalyst preparation and characterization, catalytic reaction engineering and kinetics, catalyst deactivation and industrial perspective.

Bridging Heterogeneous And Homogeneous Catalysis

Author: Can Li
Publisher: John Wiley & Sons
ISBN: 3527675922
Size: 24.69 MB
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This unique handbook fills the gap in the market for an up-to-date work that links both homogeneous catalysis applied to organic reactions and catalytic reactions on surfaces of heterogeneous catalysts.

In Situ Spectroscopy In Heterogeneous Catalysis

Author: James F. Haw
Publisher: Wiley-VCH Verlag GmbH
Size: 43.26 MB
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"Not using in-situ methods to examine catalytic processes is like studying a life with access only to the prenatal and postmortem states." This quote from the world renowned specialist in the field of in situ methods, Gabor A. Somorjai, clearly emphasizes the importance of these techniques in understanding heterogeneous catalysis - a type of chemical reaction used nowadays for most chemically produced supplies and fuels. Yet the fundamental mechanisms are often still not completely understood. Many of the leading scientists in the field have contributed to this book which provides an overview of the most varied spectroscopic and related methods for studying catalytic structures and their functions during a chemical reaction. While primarily written for users of these methods, this is also a valuable aid to interpreting the phenomena observed. Indispensable for everyone working in the field.