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Micro Reaction Technology In Organic Synthesis

Author: Charlotte Wiles
Publisher: CRC Press
ISBN: 9781439824726
Size: 75.61 MB
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While continuous processes have found widespread application within chemical production, members of the research and development communities have historically favored the centuries old technique of iterative batch reactions. With the exception of combinatorial and microwave chemistry, little had been done to change the way that synthetic chemists conduct their research. However, today’s synthetic chemist is under increasing pressure to discover and deliver compounds quickly, with an eye on devising scalable synthetic methodologies. An up-to-date account of recent developments in continuous flow organic synthesis, Micro Reaction Technology in Organic Synthesis is a useful resource for those both new to, and actively researching within, the field of micro reaction technology. Written by chemists for chemists, key synthetic information takes precedence over technological details Highlights the advantages and disadvantages of the technology, giving the reader an idea of where future research needs to be targeted Presents a comprehensive collection of synthetic reactions that have been investigated over the past decade, therefore is a one-stop resource to the reactions and techniques that have been investigated so far With an ever increasing number of commercial flow reaction platforms available, this book highlights the current state of the technology with the vision that more synthetic chemists will embark upon flow chemistry programs of research, facilitating the identification of novel synthetic methodologies the potential to be scaled directly to production.

Microreactors

Author: Wolfgang Ehrfeld
Publisher: Wiley-VCH
ISBN: 9783527295906
Size: 24.64 MB
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Tiny devices with huge potential! New concepts of chemical synthesis have led to an increasing demand for miniaturization and more complex systems. Microreaction technology is a hot topic as it opens completely new possibilities for chemical engineering, combinatorial chemistry, and biotechnology. Small, inexpensive, independent, and versatile devices ensure many reactions achieve maximum selectivity, minimum waste, minimum investment, a better control of the process, safe manufacture and production on demand - to create a more efficient process. This book outlines the fabrication techniques of microfluidic components, unit operations of micro-chemical engineering and current world-wide activities. Requirements with respect to needs of the chemical industry have been included. Chemists, chemical engineers, biotechnologists, process engineers, microsystem technologists in the chemical and pharmaceutical industry and academia, as well as manufacturers of analytical instruments, will find this book a state-of- the-art review of this extremely interesting and rapidly developing field.

Microreaction Technology

Author: M. Matlosz
Publisher: Springer Science & Business Media
ISBN: 3642567630
Size: 17.39 MB
Format: PDF
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IMRET 5 featured more than 80 oral and poster communications, covering the entire interdisciplinary field from design, production, modeling and characterization of microreactor devices to application of microstructured systems for production, energy and transportation, including many analytical and biological applications. A particularly strong topic was the investigation of the potential of microstructuring of reactors and systems components for process intensification. Perspectives of combining local, in situ, data acquisition with appropriate microstructuring of actuators and components within chemical and biological devices were explored in order to enhance process performance and facilitate process control.

Chemical Micro Process Engineering

Author: Volker Hessel
Publisher: John Wiley & Sons
ISBN: 3527606270
Size: 15.40 MB
Format: PDF, ePub, Docs
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Micro process engineering is approaching both academia and industry. With the provision of micro devices, systems and whole plants by commercial suppliers, one main barrier for using these units has been eliminated. This book focuses on processes and their plants rather than on devices: what is 'before', 'behind' and 'around' micro device fabrication - and gives a comprehensive and detailed overview on the micro-reactor plants and three topic-class applications which are mixing, fuel processing, and catalyst screening. Thus, the book reflects the current level of development from 'micro-reactor design' to 'micro-reactor process design'.

Microreaction Technology

Author: Wolfgang Ehrfeld
Publisher: Springer Science & Business Media
ISBN: 3642720765
Size: 38.32 MB
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Microreaction technology is the logically consistent application of microsystem techniques in chemical reaction and process engineering. Miniaturization in this field is the strategy of success and requires the development of small, inexpensive, independent and versatile chemical reaction units. Microreaction technology is at present regarded as one of the fastest evolving and most promising disciplines in chemical engineering, combinatorial synthesis and analysis, pharmaceutical drug development and molecular biotechnology. A broad range of microstructurable materials is a prerequisite for microreaction technology and the development of microreactors goes hand in hand with the availability of a number of modem, versatile microfabrication technologies. Today, it is possible to manufacture tbree dimensional microstructures, almost without any restrictions with regard to design and choice of suitable materials, for various chemical applications -just in time to support the development of functional units for microreactors, e. g. micromixers, micro heat exchangers, micro extractors, units for phase transfer, reaction cham bers, intelligent fluidic control elements and microanalysis systems. The advantages of microreactors, e. g. the use of novel process routes, the re duction of reaction byproducts, the improvement of 'time to market', the high flexibility for all applications requiring modular solutions, have had a strong im pact on concepts of sustainable development. Many of the leading companies and research institutes in the world have recognized the tremendous possibilities of microreactor concepts and of their economic potential, and have thus initiated worldwide research and development activities.

Basics Of Flow Microreactor Synthesis

Author: Jun-ichi Yoshida
Publisher: Springer
ISBN: 4431555137
Size: 51.54 MB
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This book provides in a concise form the principles and applications of flow microreactors in organic and polymer synthesis. Recently, it became possible to conduct chemical reactions in a flow reactor in laboratory synthesis. The flow microreactor enables reactions that cannot be done in batch, opening a new possibility of chemical synthesis. Extremely fast mass and heat transfer and high-resolution residence time control are responsible for the remarkable features of that process. The book is not an exhaustive compilation of all known examples of flow microreactor synthesis. Rather, it is a sampling of sufficient variety to illustrate the concept, the scope, and the current state of flow microreactor synthesis. Researchers both in academia and in industry will be interested in this book because the topics encompassed by the book are vigorously studied in many university and company laboratories today.

Microreaction Technology Industrial Prospects

Author: W. Ehrfeld
Publisher: Springer Science & Business Media
ISBN: 3642597386
Size: 40.30 MB
Format: PDF, ePub
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Miniaturization has cost and time-saving advantages for numerous applications in chemistry, pharmacy, medicine and biotechnology. Additionally, microreaction technology offers new solutions for the automobile industry and environmental technology, e.g. fuel cells, or mobile sensor systems for on-the-spot analysis. Therefore, the 3rd International Conference on Microreaction Technology - IMRET 3 is an important forum for creating awareness of the wide variety of the new trends in this up-and-coming discipline.

Chemical Micro Process Engineering

Author: Volker Hessel
Publisher: John Wiley & Sons
ISBN: 3527605371
Size: 24.62 MB
Format: PDF, ePub, Docs
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Micro process engineering is approaching both academia and industry. With the provision of micro devices and systems by commercial suppliers, one main barrier for using these units has been eliminated. More and more they become familiar, thereby being one facet of the upheaval in chemical industry. This book focuses on processes rather than on devices: what is 'before' and 'behind' micro device fabrication. A comprehensive and detailed overview is given on: - A multi-faceted, hierarchic analysis of chemical micro process technology - Modelling and simulation of micro reactors - Liquid- and liquid/liquid-phase reactions - Gas/liquid reactions - Gas-phase reactions (heterogeneous catalysis)

Microreactors In Organic Synthesis And Catalysis

Author: Thomas Wirth
Publisher: John Wiley & Sons
ISBN: 3527622861
Size: 40.79 MB
Format: PDF, ePub, Docs
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This one-stop reference is the first book on this emerging and rapid developing field with a focus on synthesis and catalysis. As such, it covers all aspects from academia and industry in a clearly structured way. Leading experts provide the background information as an initial aid for newcomers to the field, while chapters on different reaction types and industrial applications make this an equally vital resource for specialists.

Novel Process Windows

Author: Volker Hessel
Publisher: John Wiley & Sons
ISBN: 3527328580
Size: 58.71 MB
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This book introduces the concept of novel process windows, focusing on cost improvements, safety, energy and eco-efficiency throughout each step of the process. The first part presents the new reactor and process-related technologies, introducing the potential and benefit analysis. The core of the book details scenarios for unusual parameter sets and the new holistic and systemic approach to processing, while the final part analyses the implications for green and cost-efficient processing. With its practical approach, this is invaluable reading for those working in the pharmaceutical, fine chemicals, fuels and oils industries.