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Solving Problems With Nmr Spectroscopy

Author: Atta-ur-Rahman
Publisher: Elsevier
ISBN: 0080541496
Size: 59.80 MB
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Solving Problems with NMR Spectroscopy presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving clear examples and solutions. This text will enable organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems to work and the discussion of their solutions and interpretations will help readers becomeproficient in the application of important, modern 1D and 2D NMR techniques to structural studies. Key Features * Presents the most important NMR techniques for structural determinations * Offers a unique problem-solving approach * Uses questions and problems, including discussions of their solutions and interpretations, to help readers grasp NMR * Avoids extensive mathematical formulas * Forewords by Nobel Prize winner Richard R. Ernst and Lloyd M. Jackman

Organic Structures From Spectra

Author: L. D. Field
Publisher: John Wiley & Sons
ISBN: 1118325451
Size: 49.91 MB
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The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student’s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups. The examples themselves have been selected to include all important common structural features found in organic compounds and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. The fifth edition of this popular textbook: includes more than 250 new spectra and more than 25 completely new problems; now incorporates an expanded suite of new problems dealing with the analysis of 2D NMR spectra (COSY, C‑H Correlation spectroscopy, HMBC, NOESY and TOCSY); has been expanded and updated to reflect the new developments in NMR and to retire older techniques that are no longer in common use; provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy; features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton-coupled experiments; contains 6 problems in the style of the experimental section of a research paper and two examples of fully worked solutions. Organic Structures from Spectra, Fifth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry. Contents - Preface -Introduction - Ultraviolet Spectroscopy - Infrared Spectroscopy - Mass Spectrometry - Nuclear Magnetic Resonance Spectroscopy – 2DNMR - Problems – Index Reviews from earlier editions “Your book is becoming one of the “go to” books for teaching structure determination here in the States. Great work!” “…I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook”.—Magnetic Resonance in Chemistry “Over the past year I have trained many students using problems in your book - they initially find it as a task. But after doing 3-4 problems with all their brains activities... working out the rest of the problems become a mania. They get addicted to the problem solving and every time they solve a problem by themselves, their confident level also increases.” “I am teaching the fundamentals of Molecular Spectroscopy and your books represent excellent sources of spectroscopic problems for students.”

Annual Reports On Nmr Spectroscopy

Author: Graham A. Webb
Publisher: Academic Press
ISBN: 0080921817
Size: 58.26 MB
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The great importance of NMR in many areas of scientific research is once again highlighted in this volume of Annual Reports on NMR Spectroscopy. * Provides updates on the latest developments in NMR spectroscopy * Includes comprehensive review articles * Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

Organic Structures From 2d Nmr Spectra

Author: L. D. Field
Publisher: John Wiley & Sons
ISBN: 1118868943
Size: 34.73 MB
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The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two–dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of organic compounds. Organic Structures from 2D NMR Spectra is a carefully chosen set of more than 60 structural problems employing 2D–NMR spectroscopy. The problems are graded to develop and consolidate a student s understanding of 2D NMR spectroscopy. There are many easy problems at the beginning of the collection, to build confidence and demonstrate the basic principles from which structural information can be extracted using 2D NMR. The accompanying text is very descriptive and focussed on explaining the underlying theory at the most appropriate level to sufficiently tackle the problems. Organic Structures from 2D NMR Spectra Is a graded series of about 60 problems in 2D NMR spectroscopy that assumes a basic knowledge of organic chemistry and a basic knowledge of one–dimensional NMR spectroscopy Incorporates the basic theory behind 2D NMR and those common 2D NMR experiments that have proved most useful in solving structural problems in organic chemistry Focuses on the most common 2D NMR techniques including COSY, NOESY, HMBC, TOCSY, CH–Correlation and multiplicity–edited C–H Correlation. Incorporates several examples containing the heteronuclei 31P, 15N and 19F Organic Structures from 2D NMR Spectra is a logical follow–on from the highly successful Organic Structures from Spectra which is now in its fifth edition. The book will be invaluable for students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry. Also available: Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra

Organic Structure Determination Using 2 D Nmr Spectroscopy

Author: Jeffrey H. Simpson
Publisher: Academic Press
ISBN: 0123849705
Size: 45.90 MB
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"The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"--

Nmr Konzepte Und Methoden

Author: Daniel Canet
Publisher: Springer-Verlag
ISBN: 3642791220
Size: 61.86 MB
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Daniel Canet hat aus Seminaren und Vorlesungen an der Universität Nancy I die wesentlichen Themen der Kernresonanzspektroskopie ausgewählt. Er stellt die physikalischen Zusammenhänge so dar, daß sich eine große Gruppe für das Buch interessiert: Chemiker, Biochemiker - und auch Mediziner, in deren Diagnostik auch die spektroskopischen Aspekte eine immer größere Rolle spielen. Das Buch ist auf drei Ebenen geschrieben: als Einführung in das physikalische Phänomen, als Lehrbuch für Chemiker nach dem Vordiplom und als eine Darstellung der quantenchemischen Modelle, die zum Verständnis der Spindynamik, der Multipuls- und multidimensionalen Verfahren nötig sind. Hier unterscheidet sich Canets Buch von anderen Einführungen.

Organische Chemie

Author: Kurt Peter C. Vollhardt
Publisher: John Wiley & Sons
ISBN: 3527327541
Size: 70.20 MB
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Besser Konzepte und Ideen der organischen Chemie verstehen, als eine Vielzahl von Fakten auswendig beherrschen! Diesem Motto bleibt der "Vollhardt/Schore" auch in der neuesten Auflage treu. Das neu gestaltete Layout, beispielhaft gelöste Übungsaufgaben und die deutlich erweiterten Verständnisübungen führen einprägsam an die Methodik zur Lösung organisch-chemischer Probleme heran. So werden nicht nur die stofflichen Grundlagen der organischen Chemie, sondern auch das "Gewusst wie" fast schon spielerisch vermittelt. Nicht nur für Chemiestudenten, auch für Biochemiker, Pharmazeuten, Biologen und Mediziner ist der "Vollhardt/Schore" der fachliche Grundstock für die organische Chemie.