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Theory Of Particulate Processes

Author: Alan Randolph
Publisher: Elsevier
ISBN: 0323158498
Size: 71.83 MB
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Theory of Particulate Processes: Analysis and Techniques of Continuous Crystallization describes the complexity of crystal size distribution (CSD), secondary nucleation, and growth mechanisms. This book is divided into 10 chapters that present a generalization from CSD studies as a unified predictive theory of particulate systems. After an introduction to CSD and particle-size distribution systems, this book goes on examining several empirical, one-dimensional distribution functions suitable for the latter system. The next chapter presents a unified theory for multidimensional particle distributions which can be used to analyze and predict such distributions in certain regular, well-defined processes. These topics are followed by a survey on how the size distribution of the product of a continuous mixed-suspension, mixed product-removal crystallizer is obtained. Other chapters describe special cases, which apparently obtain in real systems, including effects of classification, poor mixing, crystal breakage, staging, and size-dependent growth. The remaining chapters deal with the ramification of secondary nucleation as contrasted with homogeneous nucleation. This book is of great value to graduate students with particulate systems course.

Crystallization Process Systems

Author: Alan G. Jones
Publisher: Butterworth-Heinemann
ISBN: 0750655208
Size: 72.55 MB
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Crystallization Process Systems gives a clear, concise, balanced and up to date presentation of crystallization and solid-liquid separation of the crystalline product. The information is presented in a coherent, concise and logical sequence based on the fundamentals of particulate crystallization processes as systems. By emphasising the analysis, design and operation of particulate crystallization processes as systems, the reader will be able to make a better judgement about the best, cheapest and most effective production method to use. Crystallization Process Systems gives a wider view and an overview of the subject of crystallization as a whole. It provides an ideal lead-in to more specialized works such as Crystallization and Solid-Liquid Separation - also published by BH. Presents a coherent, concise and logical sequence based on the fundamentals of particulate crystallization processes as systemsEmphasis on the design and optimization of the crystallization processing system

Precision Crystallization

Author: Ingo Leubner
Publisher: CRC Press
ISBN: 9781439806753
Size: 36.63 MB
Format: PDF, Kindle
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Despite the fact that crystals make up an estimated 80% of chemical and pharmaceutical products, few resources exist that provide practical guidance on achieving precision control of their size and size distribution. Based on a model developed by the author and his colleagues, Precision Crystallization: Theory and Practice of Controlling Crystal Size presents scientists and product engineers with the tools to control crystal nucleation, enabling them to ultimately control crystal size and size distribution for batch and continuous crystallizations. At the cutting edge of crystallization science and technology, this volume presents information never before available. Introducing the Balanced Nucleation and Growth (BNG) model, the book demonstrates how the results of the nucleation process are quantitatively related to practical experimental control values such as: reaction addition rate crystal solubility temperature residence time (continuous crystallizations) the effect of ripening agents (crystal supersizing) during nucleation the effect of crystal growth restrainers (crystal nanosizing) during nucleation control of renucleation The author shows how the BNG theory predicts previously unknown phenomena and also how it corrects erroneous perceptions of the importance of reaction volume on the outcome of crystal nucleation. Going above and beyond classical nucleation theories which rely to a large extent on guesswork, the BNG model gives precise guidance to scientists working in a range of critical areas, leading to promising implications for research, quality control, product development, production processes, pilot plant operations, and manufacturing.

Water Quality Engineering

Author: Mark M. Benjamin
Publisher: John Wiley & Sons
ISBN: 1118632273
Size: 22.26 MB
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Explains the fundamental theory and mathematics of water and wastewater treatment processes By carefully explaining both the underlying theory and the underlying mathematics, this text enables readers to fully grasp the fundamentals of physical and chemical treatment processes for water and wastewater. Throughout the book, the authors use detailed examples to illustrate real-world challenges and their solutions, including step-by-step mathematical calculations. Each chapter ends with a set of problems that enable readers to put their knowledge into practice by developing and analyzing complex processes for the removal of soluble and particulate materials in order to ensure the safety of our water supplies. Designed to give readers a deep understanding of how water treatment processes actually work, Water Quality Engineering explores: Application of mass balances in continuous flow systems, enabling readers to understand and predict changes in water quality Processes for removing soluble contaminants from water, including treatment of municipal and industrial wastes Processes for removing particulate materials from water Membrane processes to remove both soluble and particulate materials Following the discussion of mass balances in continuous flow systems in the first part of the book, the authors explain and analyze water treatment processes in subsequent chapters by setting forth the relevant mass balance for the process, reactor geometry, and flow pattern under consideration. With its many examples and problem sets, Water Quality Engineering is recommended as a textbook for graduate courses in physical and chemical treatment processes for water and wastewater. By drawing together the most recent research findings and industry practices, this text is also recommended for professional environmental engineers in search of a contemporary perspective on water and wastewater treatment processes.

Handbook Of Industrial Crystallization

Author: Allan Myerson
Publisher: Butterworth-Heinemann
ISBN: 9780080533513
Size: 34.53 MB
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Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes. The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design. Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the field Covers all aspects of industrial crystallization in a single, complete volume

Crystallization

Author: J W Mullin
Publisher: Elsevier
ISBN: 0080530117
Size: 20.86 MB
Format: PDF, ePub
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Since the first publication of this definitive work nearly 40 years ago, this fourth edition has been completely rewritten. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Incorporating all the recent developments and applications of crystallization technology, Crystallization gives clear accounts of the underlying principles, a review of the past and current research themes and guidelines for equipment and process design. This new edition introduces and enlarges upon such subjects as: Control and Separation of polymorphs and chiral crystals Micro- and macro-mixing and the use of computer fluid dynamics Seeding and secondary nucleation in batch crystallization processes Incorporation of upstream and downstream requirements into design procedures for crystallization plant Computer-aided molecular design and its use in crystal habit modifier selection Crystallization provides a comprehensive overview of the subject and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia. Crystallization is written with the precision and clarity of style that is John Mullin's hallmark - a special feature being the large number of appendices that provide relevant physical property data. Covers all new developments and trends in crystallization Comprehensive coverage of subject area

Recrystallization And Related Annealing Phenomena

Author: Anthony Rollett
Publisher: Newnes
ISBN: 0080982697
Size: 40.19 MB
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Recrystallization and Related Annealing Phenomena, Third Edition, fulfills the information needs of materials scientists in both industry and academia. The subjects treated in the book are all active research areas, forming a major part of at least four regular international conference series. This new third edition ensures the reader has access to the latest findings, and is essential reading to those working in the forefront of research in universities and laboratories. For those in industry, the book highlights applications of the research and technology, exploring, in particular, the significant progress made recently in key areas such as deformed state, including deformation to very large strains, the characterization of microstructures by electron backscatter diffraction, the modeling and simulation of annealing, and continuous recrystallization. Includes over 50% of new, revised, and updated material, highlighting the significant recent literature results in grain growth in non-crystallizing systems, 3D characterization techniques, quantitative modeling techniques, and all-new appendices on texture and measurements Contains synthesized, detailed coverage from leading authors that bridge the gap between theory and practice Includes a critical level of synthesis and pedagogy with an authored rather than edited volume